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Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

posted Aug 4, 2017, 1:30 AM by Daniel Lee   [ updated Oct 23, 2017, 12:40 AM ]
Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths. 2D double-quantum single-quantum correlation spectra with arbitrary spectral widths can be recorded with SR26 and related supercycled recoupling sequences when applying Supercycle-Timing-Compensation (STiC) phase shifts. This concept widely extends the applicability of supercycled sequences, most importantly for obtaining long-range distance constraints for structure determination with solid-state NMR.
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